DESY News: User operation at first PETRA III extension beamline

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2016/06/17
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User operation at first PETRA III extension beamline

The first undulator beamline of the new PETRA extension north took up regular user operation in early June. Beamline P65, offering the so-called X-ray absorption spectroscopy (EXAFS) technique, is now open to groups of scientists. Just like for the beamlines in the experimental hall “Max von Laue”, scientists have to apply for beamtime in a review process. “Three and a half years after the shutdown of DORIS we can now offer a dedicated EXAFS beamline again,” says Edmund Welter, who oversees the beamline P65. “Many researchers have been eagerly awaiting this moment.”

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Two users at the new PETRA III beamline P65 install the gas lines at the cell for catalytic samples.
In X-ray absorption spectroscopy, a sample is penetrated by X-rays, while a detector placed behind it observes which wavelengths are absorbed. Specific absorption edges are characteristic for certain chemical elements. “Based on the absorption spectrum, we can identify the chemical environment of the tested element,” says Welter. This experimental method is particularly suitable for live testing of catalysts, which are contaminated and inactived, for example by sulfur or heavy metals. Classic materials research can also be performed at P65, like the observation of the phase transition between amorphous and crystalline states in metallic glasses that are the storage medium of rewritable CDs and DVDs. “The measuring system´s design lets us investigate almost all chemical elements except those which are lighter than calcium,” says Welter. “In addition, we have a photon flux about 20 times higher than at the former DORIS beamlines, which increases the attractiveness of the beamline.”

The first users of P65 came from the Karlsruhe Institute of Technology and the University of Paderborn. With the help of the PETRA III light they checked in which way their catalyst samples age during operation, to find out what is the ideal geometry and process of application of the catalytic material on a support structure. “By means of X-ray absorption spectroscopy one can selectively improve the efficiency of industrial catalysts,” explains Edmund Welter. “For example, nowadays car catalysts include much less of the expensive noble metals than in the past, but they perform much better.”

While the beam time is assigned to the scientists at P65 until the end of the year, the other beamlines in the PETRA III extensions are built. Already this year, first experiments on the adjacent beamline P64 are supposed to be carried out. In Extension Hall East new beamlines will be put into operation in spring 2017. “With the regular user operation at P65, the expansion of PETRA III has reached an important milestone,” says Wolfgang Drube, project manager for the PETRA extensions. “We are now working flat out to build the additional beamlines, without interfering with the current user operation at the other beamlines.”